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SUN JIAXIU;SUN ZHIWEI;SHEN DECUN Institute of Atomic Energy, P. O. Box 275, Beijing. SYNTHESIS OF[1, 2-~3H] TESTOSTERONE OF HIGH SPECIFIC RADIOACTIVITY[J]. Atomic Energy Science and Technology, 1987, 21(2): 221-221. DOI: 10.7538/yzk.1987.21.02.0221
Citation: SUN JIAXIU;SUN ZHIWEI;SHEN DECUN Institute of Atomic Energy, P. O. Box 275, Beijing. SYNTHESIS OF[1, 2-~3H] TESTOSTERONE OF HIGH SPECIFIC RADIOACTIVITY[J]. Atomic Energy Science and Technology, 1987, 21(2): 221-221. DOI: 10.7538/yzk.1987.21.02.0221
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SYNTHESIS OF1, 2-~3H TESTOSTERONE OF HIGH SPECIFIC RADIOACTIVITY

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  • 1,2-~3H testosterone of specific activity as high as 51 Ci/mmol, andradiochemical purity more than 99% has been prepared. The experimental condi-tions, such as reaction time, ratio of raw material catalyst and separation methodhave been studied. The product was separated by silica-paper TLC at first, then purified byhigh performance liquid chromatography. The product has good stability with apurity of 95% after one year storage.
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