热压烧结B_4C陶瓷的力学性能研究

  • 摘要: 研究了热压烧结B4C陶瓷的室温和高温力学强度。结果表明:气流粉碎B4C粉末(中位粒径为3.85μm)在2 150℃热压烧结10 min后,烧结体密度达到理论密度的91.6%,平均晶粒尺寸为7μm,室温抗弯强度和抗压强度分别为280和1463 MPa;振动球磨B4C粉末(0.35μm)在相同条件下的热压烧结密度达到理论密度的99.7%,室温抗弯强度和抗压强度分别为515和2780 MPa。随着温度升高,两种热压烧结B4C陶瓷的抗弯强度均缓慢降低,低于600℃,抗压强度快速降低,随后则降低缓慢。对两种热压烧结B4C陶瓷的力学强度与温度、气孔率等参数之间的关系进行了讨论。

     

    Abstract: The room and high temperature mechanical strength of the hot-pressed B4C ceramic are studied. The results show that the hot-pressed B4C ceramic sintered at 2 150℃for 10 minutes from the jet-milled powders(3. 85μm), has the density of 91. 6%T. D. (T. D.--theoretic density), and the room temperature bending strength andcompression strength are 280 and 1 463 MPa, respectively. However, the hot-pressed B4C ceramic from the vibratory-milled powders(0. 35 μm) has a relative density of 99. 7% T. D., and the room temperature bending strength and compression strength are 515 and 2 870 MPa, respectively. The bending strengths of both ceramics decrease slowly with increasing temperatures, but the compression strengths decrease quickly below 600℃ and decrease slowly above 600℃. At last, the relationship between mechanical strength of both B4C ceramics and temperature and porosity is discussed by use of the empirical formulae.

     

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