氦离子辐照下金属钯薄膜的微观行为研究

Microcosmic Behavior Research of Palladium Membrane Irradiated by Helium Ions

  • 摘要: 采用电子束蒸发镀膜技术,在Si(100)面基底上沉积金属钯薄膜,并采用台阶仪和透射电子显微镜(TEM)对薄膜的厚度和结构进行表征。选取不同能量、不同剂量的氦离子束对钯薄膜进行注入实验,注入后,用X射线衍射分析(XRD)分析薄膜的微观行为。实验结果显示,在固定注入能量时,随着注入剂量的增加,钯薄膜的晶格发生膨胀,膨胀与注入造成的离位钯原子以及氦空位复合物在晶格中的存在有关。原子力显微镜(AFM)和扫描电子显微镜(SEM)的测试结果表明,由于溅射作用,薄膜表面变得略为平坦。

     

    Abstract: Palladium films were prepared on the substrate Si by electron beam evaporation, and the thickness and structure of films were characterized. Helium ions with different energies and doses were implanted in the palladium films. Through XRD analysis, it was found that the lattice was swelled when the dose of implantation was increased, and the swell was related to the existence of recoil atoms and helium-vacancy composites. The results of AFM and SEM show that the surface of films becomes flatter because of the sputtering process.

     

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