低活性F/M钢形变退火过程中的组织演化

Study on Microstructure Evolution of Deformed Low-Activation F/M Steel During Annealing

  • 摘要: 作为超临界水堆燃料包壳管用候选材料,设计和制备了一种高Cr低活性铁素体/马氏体钢(0.14C-11.06Cr-2.3W),实验钢经淬火回火热处理后为回火马氏体组织。对实验钢进行60%冷变形,并随后在750~820 ℃下退火10~720 min。通过显微组织观察和硬度测量,研究了变形前后板条马氏体在回复、再结晶、奥氏体化中的组织演化规律。结果表明,预变形既影响板条马氏体的再结晶行为,又影响奥氏体化行为。无变形的板条马氏体退火时难以发生再结晶,奥氏体直接在回火马氏体的原奥氏体晶界生成;60%预变形后易发生再结晶,奥氏体在完全再结晶的铁素体晶界上形核长大。

     

    Abstract: A new kind of high-chromium low-activation ferritic/martensitic steel (0.14C-11.06Cr-2.3W) as one of the most promising candidates for SCWR fuel cladding tube was designed and fabricated. The experimental steel after quenching-and-tempering heat treatment had a typical tempered martensitic structure. The specimens were cold-deformed by uniaxial compression to a reduction of 60% and then annealed at 750-820 ℃ for 10-720 min. The changes of matrix structure in prior cold-deformed lath martensite and softening behavior occured during annealing were investigated. The results show that the behaviors of recrystallization and austenite formation are changed by the prior deformation. The specimens without pre-deformation do not undergo recrystallization even when annealed at a rather high temperature. However, after receiving sufficiently large cold strains (60%), the deformed lath martensite easily recrystallizes. The austenite forms directly from the tempered lath martensite in the non-deformed lath martensite, when the lath martensite deforms to a reduction of 60%, the recrystallization occurs prior to austenite formation, the austenite nucleates and grows at the boundaries of completely recrystallized ferrite grains.

     

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