Cr元素对ODS合金拉伸强度的影响机制研究

Influence Mechanism of Cr Element on Tensile Strength of ODS Alloy

  • 摘要: 氧化物弥散强化(ODS)合金内部均匀分布有纳米氧化物颗粒,这种特征微观结构赋予了其优异的力学性能,使其成为第4代反应堆及聚变堆结构材料的重要候选材料而得到广泛研究。Cr元素是常见的合金添加元素,在钢中可与碳结合形成碳化物,从而提高材料的硬度、熔点及稳定性。Cr元素的含量会对ODS合金材料的显微组织结构产生一定的影响,从而改变其力学性能。因此本文针对不同Cr含量(12%Cr、14%Cr、16%Cr)的ODS铁素体合金样品,在室温及700 ℃下进行拉伸试验,通过比较其抗拉强度、延伸率、维氏显微硬度等试验结果,研究Cr含量的改变对ODS铁素体合金拉伸强度的影响,并结合其拉伸断口的SEM图像解释Cr元素对ODS铁素体合金拉伸强度的影响机制。结果发现,14Cr-ODS合金在室温或700 ℃下的抗拉强度均最高,但韧性极差;16Cr-ODS合金在700 ℃下总延伸率增加;高温下样品内韧窝更为密集且细小,韧窝内的夹杂物或第二相颗粒数目减少,因此材料在高温下强度明显下降,但塑性有所改善。

     

    Abstract: The nano-sized oxide particles are evenly dispersed in oxide dispersion strengthened (ODS) alloy. This characteristic microstructure provides the materials excellent performance, making it become an important candidate for generation Ⅳ and fusion reactors, and thus are extensively investigated. Cr is a common alloy addition elements, it can combine with carbon to form carbides in steel, thereby improving the strength, melting point and stability of the material. The content of Cr will impact the microstructure of materials and change its mechanical properties. Therefore, the effect of Cr content on the tensile strength of ODS ferrite alloy was studied in this paper, by comparing the experimental results of its tensile strength, elongation, Vickers microhardness, etc. Aiming at different Cr content (12%Cr, 14%Cr, 16%Cr) ODS ferrite alloy samples, tensile tests were carried out at room temperature and 700 ℃. The SEM images of its tensile fracture were combined to explain the influence mechanism of Cr element on the tensile strength of ODS ferrite alloy. Experiment results show that 14Cr-ODS alloy has the highest tensile strength at room temperature or 700 ℃, but its toughness is very poor. The total elongation of 16Cr-ODS alloy increases at 700 ℃, the dimples in the sample are denser and smaller at high temperatures, and the number of inclusions or second-phase particles in the dimples reduces, so the strength of the material at high temperatures decreases significantly, but plasticity improves.

     

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