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CAO DESHENG DUAN SHIRONG QIN FENGZHOU LI JINYING ZHANG HUAILI (China Institute of Atomic Energy. P. O. Box 275, Beijing. 102413). A DETERMINATION METHOD OF Ru, Rh AND Pd IN HIGH-LEVEL LIQUID WASTE(HLLW) BY CATIONEXCHANGE SEPARATION AND ICP-AES MEASUREMENT[J]. Atomic Energy Science and Technology, 1992, 26(5): 31-31. DOI: 10.7538/yzk.1992.26.05.0031
Citation: CAO DESHENG DUAN SHIRONG QIN FENGZHOU LI JINYING ZHANG HUAILI (China Institute of Atomic Energy. P. O. Box 275, Beijing. 102413). A DETERMINATION METHOD OF Ru, Rh AND Pd IN HIGH-LEVEL LIQUID WASTE(HLLW) BY CATIONEXCHANGE SEPARATION AND ICP-AES MEASUREMENT[J]. Atomic Energy Science and Technology, 1992, 26(5): 31-31. DOI: 10.7538/yzk.1992.26.05.0031
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A DETERMINATION METHOD OF Ru, Rh AND Pd IN HIGH-LEVEL LIQUID WASTE(HLLW) BY CATIONEXCHANGE SEPARATION AND ICP-AES MEASUREMENT

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  • Received Date: January 26, 1992
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  • The paper describes a determination method of Ru. Rh and Pd in HLLW with cation-exchange separation and ICP-AES measurement. A sample of HLLW was treated with the hydrochloride acid containing enough sodium chloride, then passed through a strongly acidic cation-exchange resin col umn, the Ru, Rh and Pd as ehloro-complexs go to the eluate while the interference elements are ab sorbcd on the resins in the column. The Ru, Rh and Pd are collected and determined by ICP-AES. The obtained results show that the recovery is 90％ and the relative standard deviation is 6％ as the Ru con tent within the range (35—230)×10~(-6) the recovery is 106％ and RSD is 10％ as the Rh content within (2 20)×10~(-6); and the recovery of Pd is 72％ as its content less than 2×10~6.
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    • References (6)
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    Kenawy.,I.M.Aalysis,15(6), 314(1987).
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